Sintesis dan Karakterisasi Bionano Hidroksiapatit (HAp) Secara Insitu Dengan Metode Hidrotermal
Keywords:
hydroxyapatite, pokea, hydrothermalAbstract
The pokea clamshell contains high calcium content which has the potency to be used as a precursor of calcium in synthesis of hydroxyapatite (HAp). This study aimed to utilize the waste of the pokea clamshells as a precursor of CaO in synthesizing of HAp, and to carry out the characterizations. Analysis of CaO content XRF showed that pokea clamshell after calcination was 94.23% (by weight). The hydrothermal method synthesized HAp confirmed the formation of single phase of HAp as indicated by the sharpness of the phosphate (PO43-) vibration peak at 561.85; 962.01; and 1024.55 cm-1.
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References
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[9] Oliveira, D. A., Benelli, P., and Amante, E. R. 2013. A Literature Review on Adding Value to Solid Residues: Egg Shells. Journal of Cleaner Production. 46, 42-47.
[10] Waheed S., Sultan M., Jamil T., & Hussain T., 2015. Comparative Analysis of Hydroxyapatite Synthesized by Sol-gel, Ultrasonication and Microwave Assisted Technique. In Materials Today: Proceedings,. 2(10). 17.
[11]Rodriguez-Lugo, V., Salinas-Rodriguez, E., Vazquez, R. A. Aleman, K., and Rivera, A. L., 2017. Hydroxyapatite Synthesis from A Starfish and β-Tricalcium Phosphate using a Hydrothermal Method. Royal Society of Chemistry. 7, 7631-7639.
[12] Hutabarat G. S., Qodir D. T., Setiawan H., Akbar N., & Noviyanti A. R., 2019. Sintesis Komposit Hidroksiapatit-Lantanum Oksida (HA-La2O3) dengan Metode Hidrotermal secara In-Situ dan Ex-Situ. ALCHEMY Jurnal Penelitian Kimia, 15(2), 287.
[13]Gautam, C. R., Kumar, S., Mishr, V. K., and Biradar, S., 2017. Synthesis, Structural and 3-D Architecture of Lanthanum Oxide Added Hydroxyapatite Composites for Bone Implant Applications: Enhanced Microstructural and Mechanical Properties. Ceramics International. 43, 14114–14121.
[14]Amri, M. K., Azis, Y., & Komalasari. (2019). Sintesis Hidroksiapatit dari Precipitated Calcium Carbonate (PCC) Terumbu Karang Melalui Proses Hidrotermal Dengan Variasi Rasio Ca/P Dan pH Reaksi. Jom Fteknik, (6)1.
[2] Bartonickova, E., Vojtisek, J., Tkacz, J., Porizka, J., Masilko, J., Moncekova, M., and Parizek, L., 2017. Porous HA / Alumina Composites Intended for Bone-tissue Engineering. Materiali in Tehnologije/Materials and Technology. 51, 631–636.
[3] Bozkurt,Y., Pazarlioglu, S., Gokce, H., Gurler, I., and Salman, S., 2015. Hydroxyapatite Lanthanum Oxide Composites. Acta Physica Polonica A. 127, 1407–1409.
[4] Jamarun N., Asril A., Zulhadjri, Azharman Z., & Sari T. P., 2015. Effect Of Hydrothermal Temperature On Synthesize of Hydroxyapatite From Limestone Through Hydrothermal Method. Journal of Chemical And Pharmaceutical Research, 7(6), 832–837.
[5] Sitohang, F., Yelmida, A., and Zultiniar., 2016. Sintesis Hidroksiapatit dari Precipitated Calcium Carbonate (PCC) Kulit Telur Ayam Ras Melalui Metode Hidrotermal. Jurnal Online Mahasiswa Fakultas Teknik. 3, 1-7.
[6] Maryani E., Kurniasih S. C., Sofiyaningsih, N., & Priyanto B., 2018. Penyiapan Komposit Hidroksiapatit-Zirkonia sebagai Bahan Biokeramik. Jurnal Keramik dan Gelas Indonesia, 27(1), 40-50.
[7] Ningsih R. P., Wahyuni N., & Destiarti L., 2014. Sintesis Hidroksiapatit dari Cangkang Kerang Kepah (Polymesoda erosa) dengan Variasi Waktu Pengadukan. Jurnal Kimia Khatulistiwa, 3(1), 22-26.
[8] Suwarjoyowirayatno & Ary T., 2018, Analisis Proksimat Dan Kandungan Kalsium Kerupuk Berbahan Dasar Limbah Cangkang Kerang Pokea (Batissa Violacea Celebensis Marten 1897). Analisis Proksimat dan Kandungan Kalsium, 1(1), 26–33. 16.
[9] Oliveira, D. A., Benelli, P., and Amante, E. R. 2013. A Literature Review on Adding Value to Solid Residues: Egg Shells. Journal of Cleaner Production. 46, 42-47.
[10] Waheed S., Sultan M., Jamil T., & Hussain T., 2015. Comparative Analysis of Hydroxyapatite Synthesized by Sol-gel, Ultrasonication and Microwave Assisted Technique. In Materials Today: Proceedings,. 2(10). 17.
[11]Rodriguez-Lugo, V., Salinas-Rodriguez, E., Vazquez, R. A. Aleman, K., and Rivera, A. L., 2017. Hydroxyapatite Synthesis from A Starfish and β-Tricalcium Phosphate using a Hydrothermal Method. Royal Society of Chemistry. 7, 7631-7639.
[12] Hutabarat G. S., Qodir D. T., Setiawan H., Akbar N., & Noviyanti A. R., 2019. Sintesis Komposit Hidroksiapatit-Lantanum Oksida (HA-La2O3) dengan Metode Hidrotermal secara In-Situ dan Ex-Situ. ALCHEMY Jurnal Penelitian Kimia, 15(2), 287.
[13]Gautam, C. R., Kumar, S., Mishr, V. K., and Biradar, S., 2017. Synthesis, Structural and 3-D Architecture of Lanthanum Oxide Added Hydroxyapatite Composites for Bone Implant Applications: Enhanced Microstructural and Mechanical Properties. Ceramics International. 43, 14114–14121.
[14]Amri, M. K., Azis, Y., & Komalasari. (2019). Sintesis Hidroksiapatit dari Precipitated Calcium Carbonate (PCC) Terumbu Karang Melalui Proses Hidrotermal Dengan Variasi Rasio Ca/P Dan pH Reaksi. Jom Fteknik, (6)1.
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Published
2022-07-19
How to Cite
[1]
L. A. Kadir, D. Permana, and T. . Azis, “Sintesis dan Karakterisasi Bionano Hidroksiapatit (HAp) Secara Insitu Dengan Metode Hidrotermal”, CJCS, vol. 4, no. 2, pp. 1–4, Jul. 2022.
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